Efficient Preparation of Anhydrous Metallic Triflates and Triflimides under Ultrasonic Activation
Identifieur interne : 001D27 ( Main/Repository ); précédent : 001D26; suivant : 001D28Efficient Preparation of Anhydrous Metallic Triflates and Triflimides under Ultrasonic Activation
Auteurs : RBID : Pascal:12-0234870Descripteurs français
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- Synthèse chimique, Milieu anhydre, Ultrason, Activation, Métal, Poudre, Stoechiométrie, Solvant, Catalyseur, Thiolation, Oléfine, Composé éthylénique, Arylation, Acide Lewis, Réaction sonochimique, Catalyse homogène, Bismuth, Indium III, Bismuth III, Zinc, Méthanesulfonamide(1,1,1-trifluoro-N-[(trifluorométhyl)sulfonyl]).
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Abstract
Several metallic triflates and triflimides, among them anhydrous salts, were prepared in high yields under ultrasonic activation from the corresponding metal powders and stoichiometric amounts of triflic or triflimidic acid in different solvents. Different InIII and BiIII salts were tested as catalysts in hydrothiolation of olefins and in hydroarylation processes, respectively.
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">Efficient Preparation of Anhydrous Metallic Triflates and Triflimides under Ultrasonic Activation</title><author><name sortKey="Legrave, Nathalie" uniqKey="Legrave N">Nathalie Legrave</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Institut de Chimie de Nice, Universite de Nice-Sophia Antipolis, CNRS, UMR 7272, Faculté des Sciences, Parc Valrose</s1><s2>06108 Nice</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Provence-Alpes-Côte d'Azur</region><settlement type="city">Nice</settlement></placeName></affiliation></author><author><name sortKey="Couhert, Audrey" uniqKey="Couhert A">Audrey Couhert</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Institut de Chimie de Nice, Universite de Nice-Sophia Antipolis, CNRS, UMR 7272, Faculté des Sciences, Parc Valrose</s1><s2>06108 Nice</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Provence-Alpes-Côte d'Azur</region><settlement type="city">Nice</settlement></placeName></affiliation></author><author><name sortKey="Olivero, Sandra" uniqKey="Olivero S">Sandra Olivero</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Institut de Chimie de Nice, Universite de Nice-Sophia Antipolis, CNRS, UMR 7272, Faculté des Sciences, Parc Valrose</s1><s2>06108 Nice</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Provence-Alpes-Côte d'Azur</region><settlement type="city">Nice</settlement></placeName></affiliation></author><author><name sortKey="Desmurs, Jean Roger" uniqKey="Desmurs J">Jean-Roger Desmurs</name><affiliation wicri:level="1"><inist:fA14 i1="02"><s1>CDP-Innovation, G2C Business Center, 63 rue Andre Bollier</s1><s2>Lyon</s2><s3>FRA</s3><sZ>4 aut.</sZ></inist:fA14><country>France</country><placeName><region type="région">Rhône-Alpes</region><settlement type="city">Lyon</settlement></placeName></affiliation></author><author><name sortKey="Dunach, Elisabet" uniqKey="Dunach E">Elisabet Dunach</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Institut de Chimie de Nice, Universite de Nice-Sophia Antipolis, CNRS, UMR 7272, Faculté des Sciences, Parc Valrose</s1><s2>06108 Nice</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><wicri:noRegion>06108 Nice</wicri:noRegion><wicri:noRegion>Parc Valrose</wicri:noRegion><wicri:noRegion>06108 Nice</wicri:noRegion></affiliation></author></titleStmt><publicationStmt><idno type="inist">12-0234870</idno><date when="2012">2012</date><idno type="stanalyst">PASCAL 12-0234870 INIST</idno><idno type="RBID">Pascal:12-0234870</idno><idno type="wicri:Area/Main/Corpus">001D09</idno><idno type="wicri:Area/Main/Repository">001D27</idno></publicationStmt><seriesStmt><idno type="ISSN">1434-193X</idno><title level="j" type="abbreviated">Eur. j. org. chem. : (Print)</title><title level="j" type="main">European journal of organic chemistry : (Print)</title></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Activation</term><term>Anhydrous medium</term><term>Arylation</term><term>Bismuth</term><term>Bismuth III</term><term>Catalyst</term><term>Chemical synthesis</term><term>Ethylenic compound</term><term>Homogeneous catalysis</term><term>Indium III</term><term>Lewis acid</term><term>Metal</term><term>Olefin</term><term>Powder</term><term>Solvent</term><term>Sonochemical reaction</term><term>Stoichiometry</term><term>Thiolation</term><term>Ultrasound</term><term>Zinc</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Synthèse chimique</term><term>Milieu anhydre</term><term>Ultrason</term><term>Activation</term><term>Métal</term><term>Poudre</term><term>Stoechiométrie</term><term>Solvant</term><term>Catalyseur</term><term>Thiolation</term><term>Oléfine</term><term>Composé éthylénique</term><term>Arylation</term><term>Acide Lewis</term><term>Réaction sonochimique</term><term>Catalyse homogène</term><term>Bismuth</term><term>Indium III</term><term>Bismuth III</term><term>Zinc</term><term>Méthanesulfonamide(1,1,1-trifluoro-N-[(trifluorométhyl)sulfonyl])</term></keywords><keywords scheme="Wicri" type="concept" xml:lang="fr"><term>Métal</term><term>Solvant</term><term>Bismuth</term><term>Zinc</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Several metallic triflates and triflimides, among them anhydrous salts, were prepared in high yields under ultrasonic activation from the corresponding metal powders and stoichiometric amounts of triflic or triflimidic acid in different solvents. Different In<sup>III</sup> and Bi<sup>III</sup> salts were tested as catalysts in hydrothiolation of olefins and in hydroarylation processes, respectively.</div></front></TEI><inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>1434-193X</s0></fA01><fA03 i2="1"><s0>Eur. j. org. chem. : (Print)</s0></fA03><fA06><s2>5</s2></fA06><fA08 i1="01" i2="1" l="ENG"><s1>Efficient Preparation of Anhydrous Metallic Triflates and Triflimides under Ultrasonic Activation</s1></fA08><fA11 i1="01" i2="1"><s1>LEGRAVE (Nathalie)</s1></fA11><fA11 i1="02" i2="1"><s1>COUHERT (Audrey)</s1></fA11><fA11 i1="03" i2="1"><s1>OLIVERO (Sandra)</s1></fA11><fA11 i1="04" i2="1"><s1>DESMURS (Jean-Roger)</s1></fA11><fA11 i1="05" i2="1"><s1>DUNACH (Elisabet)</s1></fA11><fA14 i1="01"><s1>Institut de Chimie de Nice, Universite de Nice-Sophia Antipolis, CNRS, UMR 7272, Faculté des Sciences, Parc Valrose</s1><s2>06108 Nice</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>5 aut.</sZ></fA14><fA14 i1="02"><s1>CDP-Innovation, G2C Business Center, 63 rue Andre Bollier</s1><s2>Lyon</s2><s3>FRA</s3><sZ>4 aut.</sZ></fA14><fA20><s1>901-904</s1></fA20><fA21><s1>2012</s1></fA21><fA23 i1="01"><s0>ENG</s0></fA23><fA43 i1="01"><s1>INIST</s1><s2>26693</s2><s5>354000508487390050</s5></fA43><fA44><s0>0000</s0><s1>© 2012 INIST-CNRS. All rights reserved.</s1></fA44><fA45><s0>16 ref.</s0></fA45><fA47 i1="01" i2="1"><s0>12-0234870</s0></fA47><fA60><s1>P</s1></fA60><fA61><s0>A</s0></fA61><fA64 i1="01" i2="1"><s0>European journal of organic chemistry : (Print)</s0></fA64><fA66 i1="01"><s0>DEU</s0></fA66><fC01 i1="01" l="ENG"><s0>Several metallic triflates and triflimides, among them anhydrous salts, were prepared in high yields under ultrasonic activation from the corresponding metal powders and stoichiometric amounts of triflic or triflimidic acid in different solvents. Different In<sup>III</sup> and Bi<sup>III</sup> salts were tested as catalysts in hydrothiolation of olefins and in hydroarylation processes, respectively.</s0></fC01><fC02 i1="01" i2="X"><s0>001C01F05</s0></fC02><fC02 i1="02" i2="X"><s0>001C01A03A</s0></fC02><fC02 i1="03" i2="X"><s0>001C01A03B</s0></fC02><fC03 i1="01" i2="X" l="FRE"><s0>Synthèse chimique</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="ENG"><s0>Chemical synthesis</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="SPA"><s0>Síntesis química</s0><s5>01</s5></fC03><fC03 i1="02" i2="X" l="FRE"><s0>Milieu anhydre</s0><s5>02</s5></fC03><fC03 i1="02" i2="X" l="ENG"><s0>Anhydrous medium</s0><s5>02</s5></fC03><fC03 i1="02" i2="X" l="SPA"><s0>Medio anhidro</s0><s5>02</s5></fC03><fC03 i1="03" i2="X" l="FRE"><s0>Ultrason</s0><s5>03</s5></fC03><fC03 i1="03" i2="X" l="ENG"><s0>Ultrasound</s0><s5>03</s5></fC03><fC03 i1="03" i2="X" l="SPA"><s0>Ultrasonido</s0><s5>03</s5></fC03><fC03 i1="04" i2="X" l="FRE"><s0>Activation</s0><s5>04</s5></fC03><fC03 i1="04" i2="X" l="ENG"><s0>Activation</s0><s5>04</s5></fC03><fC03 i1="04" i2="X" l="SPA"><s0>Activación</s0><s5>04</s5></fC03><fC03 i1="05" i2="X" l="FRE"><s0>Métal</s0><s2>NC</s2><s5>05</s5></fC03><fC03 i1="05" i2="X" l="ENG"><s0>Metal</s0><s2>NC</s2><s5>05</s5></fC03><fC03 i1="05" i2="X" l="SPA"><s0>Metal</s0><s2>NC</s2><s5>05</s5></fC03><fC03 i1="06" i2="X" l="FRE"><s0>Poudre</s0><s5>06</s5></fC03><fC03 i1="06" i2="X" l="ENG"><s0>Powder</s0><s5>06</s5></fC03><fC03 i1="06" i2="X" l="SPA"><s0>Polvo</s0><s5>06</s5></fC03><fC03 i1="07" i2="X" l="FRE"><s0>Stoechiométrie</s0><s5>07</s5></fC03><fC03 i1="07" i2="X" l="ENG"><s0>Stoichiometry</s0><s5>07</s5></fC03><fC03 i1="07" i2="X" l="SPA"><s0>Estequiométría</s0><s5>07</s5></fC03><fC03 i1="08" i2="X" l="FRE"><s0>Solvant</s0><s5>08</s5></fC03><fC03 i1="08" i2="X" l="ENG"><s0>Solvent</s0><s5>08</s5></fC03><fC03 i1="08" i2="X" l="SPA"><s0>Solvente</s0><s5>08</s5></fC03><fC03 i1="09" i2="X" l="FRE"><s0>Catalyseur</s0><s5>09</s5></fC03><fC03 i1="09" i2="X" l="ENG"><s0>Catalyst</s0><s5>09</s5></fC03><fC03 i1="09" i2="X" l="SPA"><s0>Catalizador</s0><s5>09</s5></fC03><fC03 i1="10" i2="X" l="FRE"><s0>Thiolation</s0><s5>10</s5></fC03><fC03 i1="10" i2="X" l="ENG"><s0>Thiolation</s0><s5>10</s5></fC03><fC03 i1="10" i2="X" l="SPA"><s0>Tiolación</s0><s5>10</s5></fC03><fC03 i1="11" i2="X" l="FRE"><s0>Oléfine</s0><s5>11</s5></fC03><fC03 i1="11" i2="X" l="ENG"><s0>Olefin</s0><s5>11</s5></fC03><fC03 i1="11" i2="X" l="SPA"><s0>Olefina</s0><s5>11</s5></fC03><fC03 i1="12" i2="X" l="FRE"><s0>Composé éthylénique</s0><s5>12</s5></fC03><fC03 i1="12" i2="X" l="ENG"><s0>Ethylenic compound</s0><s5>12</s5></fC03><fC03 i1="12" i2="X" l="SPA"><s0>Compuesto etilénico</s0><s5>12</s5></fC03><fC03 i1="13" i2="X" l="FRE"><s0>Arylation</s0><s5>13</s5></fC03><fC03 i1="13" i2="X" l="ENG"><s0>Arylation</s0><s5>13</s5></fC03><fC03 i1="13" i2="X" l="SPA"><s0>Arilación</s0><s5>13</s5></fC03><fC03 i1="14" i2="X" l="FRE"><s0>Acide Lewis</s0><s5>14</s5></fC03><fC03 i1="14" i2="X" l="ENG"><s0>Lewis acid</s0><s5>14</s5></fC03><fC03 i1="14" i2="X" l="SPA"><s0>Acido Lewis</s0><s5>14</s5></fC03><fC03 i1="15" i2="X" l="FRE"><s0>Réaction sonochimique</s0><s5>15</s5></fC03><fC03 i1="15" i2="X" l="ENG"><s0>Sonochemical reaction</s0><s5>15</s5></fC03><fC03 i1="15" i2="X" l="SPA"><s0>Reacción sonoquímica</s0><s5>15</s5></fC03><fC03 i1="16" i2="X" l="FRE"><s0>Catalyse homogène</s0><s5>16</s5></fC03><fC03 i1="16" i2="X" l="ENG"><s0>Homogeneous catalysis</s0><s5>16</s5></fC03><fC03 i1="16" i2="X" l="SPA"><s0>Catálisis homogénea</s0><s5>16</s5></fC03><fC03 i1="17" i2="X" l="FRE"><s0>Bismuth</s0><s2>NC</s2><s5>17</s5></fC03><fC03 i1="17" i2="X" l="ENG"><s0>Bismuth</s0><s2>NC</s2><s5>17</s5></fC03><fC03 i1="17" i2="X" l="SPA"><s0>Bismuto</s0><s2>NC</s2><s5>17</s5></fC03><fC03 i1="18" i2="X" l="FRE"><s0>Indium III</s0><s2>NC</s2><s5>18</s5></fC03><fC03 i1="18" i2="X" l="ENG"><s0>Indium III</s0><s2>NC</s2><s5>18</s5></fC03><fC03 i1="18" i2="X" l="SPA"><s0>Indio III</s0><s2>NC</s2><s5>18</s5></fC03><fC03 i1="19" i2="X" l="FRE"><s0>Bismuth III</s0><s2>NC</s2><s5>19</s5></fC03><fC03 i1="19" i2="X" l="ENG"><s0>Bismuth III</s0><s2>NC</s2><s5>19</s5></fC03><fC03 i1="19" i2="X" l="SPA"><s0>Bismuto III</s0><s2>NC</s2><s5>19</s5></fC03><fC03 i1="20" i2="X" l="FRE"><s0>Zinc</s0><s2>NC</s2><s5>20</s5></fC03><fC03 i1="20" i2="X" l="ENG"><s0>Zinc</s0><s2>NC</s2><s5>20</s5></fC03><fC03 i1="20" i2="X" l="SPA"><s0>Zinc</s0><s2>NC</s2><s5>20</s5></fC03><fC03 i1="21" i2="X" l="FRE"><s0>Méthanesulfonamide(1,1,1-trifluoro-N-[(trifluorométhyl)sulfonyl])</s0><s4>INC</s4><s5>62</s5></fC03><fC07 i1="01" i2="X" l="FRE"><s0>Métal transition</s0><s2>NC</s2><s5>51</s5></fC07><fC07 i1="01" i2="X" l="ENG"><s0>Transition metal</s0><s2>NC</s2><s5>51</s5></fC07><fC07 i1="01" i2="X" l="SPA"><s0>Metal transición</s0><s2>NC</s2><s5>51</s5></fC07><fN21><s1>177</s1></fN21></pA></standard></inist></record>Pour manipuler ce document sous Unix (Dilib)
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